Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19838104 | HCID 19838104 | — |
| Product | HCID 19838231 | HCID 19838231 | — |
Reaction Steps
A solution of N-[2-[3,4-Bis(phenylmethoxy)phenyl]ethyl]-2,2,2-trifluoroacetamide (11 g) in dry dimethylformamide (30 ml) was added dropwise to a stirred suspension of sodium hydride (0.615 g) in dry dimethylformamide (20 ml) in (a) nitrogen atmosphere. The mixture was heated at 70° C. for 1 hour and then cooled to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04803225 |
|---|
| Source dataset | uspto-grants-1989_02 |
|---|
| ORD ID | ord-ced21b9873364c2b9edfbdaef9b4d254 |
|---|
| Source note | uspto-grants-1989_02 |
|---|
