Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Reactant | HCID 14350448 | HCID 14350448 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10376130 | HCID 10376130 | — |
Reaction Steps
In 100 ml water is dissolved 29.0 g (0.11 mol) of 1-(4-pyridyl)-1-hydroxy-2-amino-3-ketopentane dihydrochloride and 17.9 g (0.22 mol) of potassium cyanate. The solution is warmed to 50° C. for 10 minutes and then allowed to stand at room temperature for 10 hours, cooled and the solid collected to give the title compound; m.p. 234°-36°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04803278 |
|---|
| Source dataset | uspto-grants-1989_02 |
|---|
| ORD ID | ord-f58775c30126458d840a18ae5394aa01 |
|---|
| Source note | uspto-grants-1989_02 |
|---|
