Water → HCID 21276535, compound

Participants

Reaction Steps

335 mg of product from Example 9 was dissolved in 10 ml of methylene chloride and 10 ml of trifluroacetic acid was added. The reaction mixture was stirred at room temperature for 1.5 hours and added to 20 ml of water. The organic layer was separated and dried over sodium sulfate. The solvent was removed using a rotary evaporator to give 270 mg of the titled product.

Provenance & Evidence