Lithium hydroxide, monohydrate → HCID 15592211, compound

HRID 1381721Notes

Reaction equation

HRID 1381721 reaction equation
[Cl:1][C:2]1[CH:11]=[C:10]([C:12](=[O:30])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[CH:9]=[CH:8][C:3]=1[C:4]([O:6]C)=[O:5].O.[OH-].[Li+]>>[Cl:1][C:2]1[CH:11]=[C:10]([C:12](=[O:30])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[CH:9]=[CH:8][C:3]=1[C:4]([OH:6])=[O:5]

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 21276537HCID 21276537, compound

Product 1

HCID 15592211HCID 15592211, compound

Procedure

By the method of Example 11, 320 mg of the product of Example 14 was treated with 200 mg of lithium hydroxide monohydrate to give the product of Example 11, the title compound.

Sources & evidence

ORD record
ord-97db85a30d2445aab0861127264139f9
Source dataset
uspto-grants-1989_02
Patent number
US04803294

Reaction notes

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