Iodoethane → HCID 13375401, compound

HRID 1381780Notes

Reaction equation

HRID 1381780 reaction equation
[CH3:1][S:2][C:3]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[C:10]([CH:17]=[O:18])=[C:9]2[C:4]=1[CH:5]=[CH:6][CH:7]=[CH:8]2.Cl[C:20]1C2C(=CC=CC=2)C(C=O)=C2C=1C=CC=C2.C(I)C>>[CH2:1]([S:2][C:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[C:10]([CH:17]=[O:18])=[C:11]2[C:16]=1[CH:15]=[CH:14][CH:13]=[CH:12]2)[CH3:20]

Participants

4

Reactant 3

HCID 6340IodoethaneHCID 8270310-Chloro-9-anthraldehydeHCID 13375392HCID 13375392, compound

Product 1

HCID 13375401HCID 13375401, compound

Procedure

Using the procedure described in 3A, 10-chloro-9-anthracenecarbaldehyde (Aldrich) and ethyl iodide (Fisher) gave an oil which solidified to give 10-ethylthio-9-anthracenecarbaldehyde mp 74°-75.5° (C, H, S).

Workup

  1. customgave an oil which

Sources & evidence

ORD record
ord-c7e97c2842394660aab4f05215cb9cb9
Source dataset
uspto-grants-1989_02
Patent number
US04803221

Reaction notes

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