HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21275487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21275473 | HCID 21275473 | — |
| Product | HCID 21275487 | HCID 21275487 | 82.2% |
Reaction Steps
A mixture of 2,2-dimethoxy-5-methyl-6-(2-thiazolyl)-2H-1,4-thiazin-3-(4H)-one (80 mg) and 2N hydrochloric acid solution (2 ml) was stirred at room temperature for 6 hours. Then the mixture was neutralized with saturated sodium bicarbonated aqueous solution and the resulting precipitates were collected to give methyl 4-methyl-5-(2-thiazolyl)-thiazole-2-carboxylate (58 mg, yield 82.2%) as colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04804668 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-add21d9b0a42484bb671eb76c032a7e9 |
| Source note | uspto-grants-1989_02 |