Oxalyl chloride → HCID 21275659, compound

HRID 1381924Notes

Reaction equation

HRID 1381924 reaction equation
[CH3:1][O:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[C:5]([O:13][CH3:14])[C:4]=1[C:15]([OH:17])=O.C(Cl)(=O)C([Cl:21])=O>>[CH3:1][O:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[C:5]([O:13][CH3:14])[C:4]=1[C:15]([Cl:21])=[O:17]

Participants

3

Reactant 2

HCID 65578Oxalyl chlorideHCID 13923894HCID 13923894, compound

Product 1

HCID 21275659HCID 21275659, compound

Procedure

The product is prepared from 9.28 g. (40 mmoles) of 1,3-dimethoxy-2-naphthoic acid and 10.15 g. (80 mmoles) of oxalyl chloride by the process of Step 3 of Example 1.

Workup

  1. customThe product is prepared from 9.28 g

Sources & evidence

ORD record
ord-f50d7af8da7e4703b12faa694c3ae64a
Source dataset
uspto-grants-1989_02
Patent number
US04804679

Reaction notes

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