HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 14253456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Propanenitrile, 3-(methylamino)- | HCID 69656 | — |
| Reactant | 2-Chloropyridine-4-carbonyl chloride | HCID 2800003 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14253456 | HCID 14253456 | — |
Reaction Steps
2 g (0.0136 mol) of 2-chloroisonicotinoyl chloride was added dropwise to a solution comprising 1.2 g (0.01136 mol) of N-methyl-N-(2-cyanoethyl)amine, 1.9 ml (0.0136 mol) of triethylamine and 30 ml of acetonitrile under cooling at 5° to 10° C. The mixture was stirred at room temperature for 2 h and then poured into water. Ethyl acetate was added thereto to conduct extraction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04804762 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-34b8653632054d0796eef6eeabe4221b |
| Source note | uspto-grants-1989_02 |