HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1381992Generated: October 26, 2026
Sulfuric Acid → 2,4-Dichloro-3-methyl-5-nitrobenzoic acid
https://huagongshe.com/reaction/1381992
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Potassium Nitrate | HCID 24434 | — |
| Reactant | 2,4-Dichloro-3-methylbenzoic acid | HCID 13235951 | — |
| Product | 2,4-Dichloro-3-methyl-5-nitrobenzoic acid | HCID 13657443 | — |
Reaction Steps
30 g of 2,4-dichloro-3-methylbenzoic acid are initially introduced into 83 ml of concentrated H2SO4. 16.7 g of KNO3 are added in portions with ice cooling. The mixture is subsequently warmed at 50° C. for a further 2 hours and then poured onto ice. The nitro compound is isolated and recrystallized from toluene. Melting point 152°-4° C., yield: 24 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04804760 |
|---|
| Source dataset | uspto-grants-1989_02 |
|---|
| ORD ID | ord-18b6946b2fdd45618207f6e8a407d1fb |
|---|
| Source note | uspto-grants-1989_02 |
|---|
