HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → HCID 178472080, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Ethyl 2-(2,4-dichloro-5-fluoro-3-nitrobenzoyl)-3-ethoxyacrylate | HCID 53944414 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178472080 | HCID 178472080 | — |
Reaktionsschritte
38 g of the product from Example 1 are intitially introduced into 40 ml of ethanol. A mixture of 8 ml of concentrated NH3 solution in 25 ml of ethanol is added dropwise with ice cooling. The mixture is stirred for 2 hours at room temperature and the phases are then separated. The organic phase is washed with water and dried. 38.3 g of the title compound remain on concentration.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04804760 |
| Quelldatensatz | uspto-grants-1989_02 |
| ORD ID | ord-a0a1df0fb3fa461bad80ef8c291d42ba |
| Quellennotiz | uspto-grants-1989_02 |