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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1382001Erstellt: 25. Oktober 2026

Ammonia → HCID 178472080, Verbindung

https://huagongshe.com/reaction/1382001

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAmmoniaHCID 222—
EduktEthyl 2-(2,4-dichloro-5-fluoro-3-nitrobenzoyl)-3-ethoxyacrylateHCID 53944414—
LösungsmittelEthanolHCID 702—
ProduktHCID 178472080HCID 178472080—

Reaktionsschritte

38 g of the product from Example 1 are intitially introduced into 40 ml of ethanol. A mixture of 8 ml of concentrated NH3 solution in 25 ml of ethanol is added dropwise with ice cooling. The mixture is stirred for 2 hours at room temperature and the phases are then separated. The organic phase is washed with water and dried. 38.3 g of the title compound remain on concentration.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04804760
Quelldatensatzuspto-grants-1989_02
ORD IDord-a0a1df0fb3fa461bad80ef8c291d42ba
Quellennotizuspto-grants-1989_02