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HRID1382156

反应详情

EQUATION

反应方程式

HRID 1382156 的结构方程式

REACTANTS

反应物

1
结构：CC(C)Oc1cc(-n2nc(C(F)F)n(C)c2=O)c(Cl)cc1Cl
HCID14392486

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(C(F)F)nn(-c2cc(O)c(Cl)cc2Cl)c1=O
HCID14392487

未命名化合物

收率 71.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=S(=O)(O)O
溶剂HCID1118

Sulfuric acid

H2O4S

PROCEDURE

实验过程

Hydrolysis of 2.2 g (0.0063 mole) of 1-[2,4-dichloro-5-(1-methylethoxy)phenyl]-3-difluoromethyl-4,5-dihydro-4-methyl-1,2,4-triazol-5(1H)-one in 5 mL of concentrated sulfuric acid produced 1.4 g of 1-(2,4-dichloro-5-hydroxyphenyl)-3-difluoromethyl-4,5-dihydro-4-methyl-1,2,4-triazol-5(1H)-one (mp 176°-179° C.).