P-Cresol → HCID 14422831, compound

HRID 1382383Notes

Reaction equation

HRID 1382383 reaction equation
Cl[CH2:2][CH:3]([OH:7])[CH2:4][CH2:5][Cl:6].[CH3:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1>>[Cl:6][CH2:5][CH2:4][CH:3]([OH:7])[CH2:2][O:15][C:12]1[CH:13]=[CH:14][C:9]([CH3:8])=[CH:10][CH:11]=1

Participants

3

Reactant 2

HCID 2879P-CresolHCID 170211,4-Dichloro-2-butanol

Product 1

HCID 14422831HCID 14422831, compoundYield 42%

Procedure

Utilizing the procedure of Preparation 21, 1,4-dichloro-2-butanol was reacted with 4-methylphenol to give white title compound, m.p. 62°-64° C. in 42% yield.

Sources & evidence

ORD record
ord-737c1764e3fc4a6f8b29caf787620728
Source dataset
uspto-grants-1989_02
Patent number
US04806555

Reaction notes

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