HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylpiperazine → HCID 14422859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-Butanol, 4-chloro-1-[3-(trifluoromethyl)phenoxy]- | HCID 13120348 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 14422859 | HCID 14422859 | 42.3% |
Reaction Steps
This compound was prepared according to the procedure of Example 78. A mixture of 2.4 g (0.015 mole) of 1-phenylpiperazine, 4.0 g (0.015 mole) of 4-chloro-1-(3-trifluoromethylphenoxy)-2-butanol and 5.3 g (0.05 mole) of anhydrous sodium carbonate in 100 ml of 1-butanol gave 2.5 g (42%) of a tan powder, m.p. 73°-74° C. Recrystallizing solvent used was ligroin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04806555 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-b824cadb4d9d4d5eb95aeb306fe5b09f |
| Source note | uspto-grants-1989_02 |