Potassium Iodide → HCID 14422900, compound

Participants

Reaction Steps

This compound was prepared according to the procedure of Example 97. A mixture of 6.8 g (0.03 mole) of 4-chloro-1-(4-cyanophenoxy)-2-butanol, 4.9 g (0.03 mole) of 1-phenylpiperazine, 16.0 g (0.15 mole) of anhydrous sodium carbonate and 0.3 g (0.002 mole) of potassium iodide in a total volume of 200 ml of 1-butanol gave an oil as residue. The hydrochloric acid salt was formed in ethereal hydrogen chloride and the collected solid was recrystallized from methanolethyl ether to give 3.7 g (35%) of white solid, m.p. 195°-198° C.

Provenance & Evidence