HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile, 4-bromo- → HCID 19786992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile, 4-bromo- | HCID 12162 | — |
| Reactant | HCID 19786988 | HCID 19786988 | — |
| Product | HCID 19786992 | HCID 19786992 | — |
Reaction Steps
Using a process similar to that described in Example 1c, 4.4 g (22 millimoles) of (5,6,7,8-tetrahydro-3,8,8-trimethylnaphth-2-yl)-ethyne and 2.7 g (15 millimoles) of 4-bromobenzonitrile were converted to the title compound. 1.3 g (29%) of product of melting point 128°-130° C. were obtained after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04806558 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-7198b93e7d28476fa86bfbf126133639 |
| Source note | uspto-grants-1989_02 |