HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54504884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | HCID 19853728 | HCID 19853728 | — |
| Reactant | HCID 54096058 | HCID 54096058 | — |
| Catalyst | Nickel Acetate | HCID 9756 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54504884 | HCID 54504884 | — |
Reaction Steps
The procedure is the same for 3-ethynylphenyl maleimide. The following amounts of staring materials were used: 4-butenyloxyaniline (4.0 g, 24.5 mmol), maleic anhydride (2.4 g, 24.5 mmol), acetone (100 ml) triethylamine (5 ml), nickel (II) acetate (0.25 g, 3.5 mmol), and acetic anhydride (2.75 g, 27 mmol). Yield=5.0 g, (84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04806608 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-e659dd84eb1e4d769ecb2b614e3dc117 |
| Source note | uspto-grants-1989_02 |