HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 13292773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 13292770 | HCID 13292770 | — |
| Product | HCID 13292773 | HCID 13292773 | 82.4% |
Reaction Steps
A mixture of 3.34 g (7.5 mmoles) of (E)-1-[4-(2-bromoethoxy)-phenyl]-1,2-diphenyl-3,3,3-trifluoro-propene, prepared as described in Example 7, and 13 g of morpholine is boiled for one hour. The reaction mixture is processed as described in Example 1, and the crude product is crystallized from hexane. 2.80 g (82.4%) of the aimed compound are obtained; m.p.: 84°-89° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04806685 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-179309e8afc44b1093e21edddd2b1c6f |
| Source note | uspto-grants-1989_02 |