HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 14350502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 14350500 | HCID 14350500 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14350502 | HCID 14350502 | — |
Reaction Steps
A 1.0 g portion of 2-(4-chlorophenyl)-4,7-dimethoxy-1H-benzimidazole, 1.40 g of aluminum chloride and 50 ml of toluene was heated at reflux for 2 hours, then cooled and poured into cold 3N hydrochloric acid. The resulting solid was collected and recrystallized from ethanol, giving 680 mg of the desired product, mp>300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808586 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-be80c0c0f7db4c64b2da912c059ac3c6 |
| Source note | uspto-grants-1989_02 |