HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-oxocyclohexylacetate → 9-p-Chlorobenzyl-6,8-dimethyl-1,2,3,4-tetrahydrocarbazol-1-yl-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-oxocyclohexylacetate | HCID 91229 | — |
| Reactant | 2,4-Dimethylphenylhydrazine hydrochloride | HCID 16213059 | — |
| Product | 9-p-Chlorobenzyl-6,8-dimethyl-1,2,3,4-tetrahydrocarbazol-1-yl-acetic acid | HCID 14372506 | — |
Reaction Steps
Following the procedure of Example 34, but using 1-(2,4-dimethylphenyl)hydrazine hydrochloride and ethyl 2-cyclohexanone acetate in Step I as starting materials, the title compound was prepared. m.p. 187°-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808608 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-ee9faac5eb0d48ab81ae57cfcebc1ed0 |
| Source note | uspto-grants-1989_02 |