HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → 3-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-(3-chloropropyl)-1H-pyrazolo[3,4-b]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | HCID 178440702 | HCID 178440702 | — |
| Product | 3-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-(3-chloropropyl)-1H-pyrazolo[3,4-b]pyridine | HCID 136151016 | — |
Reaction Steps
3-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-(3-chloropropyl)-1H-pyrazolo[3,4-b]pyridine, melting at 107°-109° C. is prepared by reacting the compound of Example 1 with 3-chloropropyl bromide in a similar manner as Example 9, and recrystallizing from acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808620 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-8509bc911bdd403486033f3e69f8a3d3 |
| Source note | uspto-grants-1989_02 |