HRID1382887

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

结构：CC(C)(C)c1cc(-c2n[nH]c3ncccc23)cc(C(C)(C)C)c1O

HCID178440702

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)c1cc(-c2nn(CCCCl)c3ncccc23)cc(C(C)(C)C)c1O

HCID136151016

未命名化合物

PROCEDURE

实验过程

3-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-(3-chloropropyl)-1H-pyrazolo[3,4-b]pyridine, melting at 107°-109° C. is prepared by reacting the compound of Example 1 with 3-chloropropyl bromide in a similar manner as Example 9, and recrystallizing from acetonitrile.

WORKUP

后处理

customrecrystallizing from acetonitrile