HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86742774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86742775 | HCID 86742775 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86742774 | HCID 86742774 | 89.5% |
Reaction Steps
89 g (374 mmol) of tert.butyl (S)-6-aminoheptanoate hydrochloride are dissolved in 1.3 l of methylene chloride. The solution is saturated with hydrogen chloride and heated to reflux for 4 hours. After filtering off and drying the precipitate formed there are obtained 60.8 g (89.5%) of (S)-6-aminoheptanoic acid hydrochloride, m.p. 157°-160°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808605 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-abde772deaed45efb80e78c9d02fc97f |
| Source note | uspto-grants-1989_02 |