HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12237176, compound → HCID 14372148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12237176 | HCID 12237176 | — |
| Reactant | 4-chloro-6-methylfuro[3,2-c]pyridine | HCID 12237184 | — |
| Reactant | HCID 14372147 | HCID 14372147 | — |
| Product | HCID 14372148 | HCID 14372148 | — |
Reaction Steps
The title compound was prepared according to the procedure described for 4-chloro-6-methylfuro[3,2-c]pyridine (Example 12, Step B) except 7-methylfuro[3,2-c]pyridin-4-(5H)-one was substituted for 6-methylfuro[3,2-c]pyridin-4-(5H)-one. Title compound was obtained in 98% crude yield and used as is. A portion was crystallized from cold diethyl ether for microanalysis, mp. 51.5°-53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808595 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-1c409d913b1d489db360b8fae7b353fe |
| Source note | uspto-grants-1989_02 |