Sodium Bicarbonate → HCID 70393745, compound

HRID 1383114Notes

Reaction equation

C([O-])(=O)C.[CH3:5][N:6]([CH3:34])[C:7]1[CH:33]=[CH:32][C:10]([CH:11]=[N:12][N+:13]2[CH:17]=[CH:16][N:15]([N:18]=[CH:19][C:20]3[CH:25]=[CH:24][C:23]([N:26]([CH3:28])[CH3:27])=[CH:22][CH:21]=3)[C:14]=2[CH:29]([CH3:31])[CH3:30])=[CH:9][CH:8]=1.[C:35](=[O:38])([O-:37])[OH:36].[Na+]>>[C:35](=[O:36])([O-:38])[OH:37].[CH3:28][N:26]([CH3:27])[C:23]1[CH:22]=[CH:21][C:20]([CH:19]=[N:18][N+:15]2[CH:16]=[CH:17][N:13]([N:12]=[CH:11][C:10]3[CH:32]=[CH:33][C:7]([N:6]([CH3:5])[CH3:34])=[CH:8][CH:9]=3)[C:14]=2[CH:29]([CH3:31])[CH3:30])=[CH:25][CH:24]=1

Participants

Reactant 2

HCID 516892Sodium Bicarbonate

HCID 70393775HCID 70393775, compound

Product 1

HCID 70393745HCID 70393745, compound

Procedure

25 mg of 1,3-bis[[p-(dimethylamino)benzylidene]amino]-2-isopropylimidazolium acetate are suspended in 5 ml of saturated sodium hydrogen carbonate solution. After stirring for three days the product is filtered and washed with water. There is obtained 1,3-bis[[p-(dimethylamino)benzylidene]amino]-2-isopropylimidazolium hydrogen carbonate of melting point 122°-124°.

Workup

filtrationis filtered
washwashed with water

Sources & evidence

ORD record: ord-43d43325ca10480fbc40bdda1bcd8a8e
Source dataset: uspto-grants-1989_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04808727

Reaction notes

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