HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → 4-[[[5-(4-Acetyl-3-hydroxy-2-propylphenoxy)pentyl]thio]methyl]-1,3-oxathiolane-2,2-dipropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Diethyl 4-[[[5-(4-acetyl-3-hydroxy-2-propylphenoxy)pentyl]thio]methyl]-1,3-oxathiolane-2,2-dipropanoate | HCID 14405889 | — |
| Product | 4-[[[5-(4-Acetyl-3-hydroxy-2-propylphenoxy)pentyl]thio]methyl]-1,3-oxathiolane-2,2-dipropanoic acid | HCID 14405890 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 3 using the ester produced in Example 4 (1.0 g, 0.0016 mol) and aqueous lithium hydroxide solution (2 M, 3.0 ml). Following the workup procedure of Example 3, 0.99 g (96%) of the product was obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808729 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-0ae5d8ea350e4066a1bccdbc9c21f9d8 |
| Source note | uspto-grants-1989_02 |