HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14405913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-[4-(3-bromopropoxy)-2-hydroxy-3-propylphenyl]ethanone | HCID 2775221 | — |
| Reactant | HCID 14405953 | HCID 14405953 | — |
| Product | HCID 14405913 | HCID 14405913 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 2 using the mercaptan produced in Example 36 (1.5 g, 0.006 mol), 3-(2-n-propyl-3-hydroxy-4-acetylphenoxy)-1-bromopropane (1.9 g, 0.006 mol) and anhydrous potassium carbonate (2.5 g). The crude product was chromatographed on silica gel using 20% ethyl acetate/hexane as eluent to give 2.7 g (93%) of the product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808729 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-ec6ec98142e14b21b6396d36d65ad56d |
| Source note | uspto-grants-1989_02 |