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HRID1383248

反应详情

EQUATION

反应方程式

HRID 1383248 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：CC(=O)NC1CC(C)(C)N(O)C(C)(C)C1
HCID579904

N-(1-Hydroxy-2,2,6,6-tetramethylpiperidin-4-yl)acetamide

C11H22N2O2

PRODUCTS

生成物

1
结构：CC(=O)NC1CC(C)(C)[NH+](O)C(C)(C)C1.O=S(=O)([O-])O
HCID22182980

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

2.6 ml of concentrated sulfuric acid is added dropwise to a solution of 10.0 g (46.9 mmol) 1-oxyl-2,2,6,6-tetramethyl-4-acetamidopiperidine in 50 ml isopropanol. After 48 hrs the resulting white solid is collected by filtration, washed with isopropanol and dried under vacuum, mp 198° C.

WORKUP

后处理

  1. filtrationAfter 48 hrs the resulting white solid is collected by filtration
  2. washwashed with isopropanol
  3. customdried under vacuum, mp 198° C.