HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54385380, compound → HCID 21042177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54385380 | HCID 54385380 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21042177 | HCID 21042177 | 92.9% |
Reaction Steps
28 g (0.11 mol) of 7-methyloxacyclohexadec-6-en-2-one were dissolved in 200 ml of ethyl acetate and hydrogenated in the presence of 2 g of 5% palladium-on-carbon under 150 mbar of hydrogen. The mixture was filtered over Celite, concentrated and distilled in a bulb-tube. 26 g (92%) of 7-methyloxacyclohexadecan-2-one were obtained having the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255276B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-d10a067371394e8ab533a2cbe5eed4d6 |
| Source note | uspto-grants-2001_07 |