HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 10921895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Methyl 4-amino-5-chloro-2-methoxybenzoate | HCID 700493 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10921895 | HCID 10921895 | — |
Reaction Steps
51.5 g (0.239 mol) of methyl 4-amino-5-chloro-2-methoxybenzoate suspended in 460 ml of ethanol are introduced into a 1 l reactor. 119 g (2.39 mol) of hydrazine hydrate are added, over 15 min, and the mixture is refluxed for 15 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255319B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-d96cd2a7b11d477ca1a86d318fafecef |
| Source note | uspto-grants-2001_07 |