HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21188020, compound → Phenol, 2-(2-phenyl-5-oxazolyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21188020 | HCID 21188020 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Phenol, 2-(2-phenyl-5-oxazolyl)- | HCID 11128316 | — |
Reaction Steps
0.55 g of 5-(2-benzyloxyphenyl)-2-phenyl-1,3-oxazole according to step (c) are hydrogenated in 30 ml of tetrahydrofuran in the presence of 0.1 g of Pd/C catalyst (10W) at about 60° C. (5.7 bar). After the catalyst has been separated off the solvent is distilled off in vacuo and the residue remaining is chromatographed on silica gel (dioxane:hexane 3:5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255327B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-2413310354814fb29d6a8830e629cc77 |
| Source note | uspto-grants-2001_07 |