HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15391352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86757109 | HCID 86757109 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15391352 | HCID 15391352 | 103% |
Reaction Steps
3.0 g (7 mmol) of the compound from Example I are dissolved in 14 ml of dioxane, treated with 2 ml of conc. HCl and the solution is refluxed for 5 h. It is concentrated, the residue is taken up in CH2Cl2 and the solution is washed with water. 2.6 g (96%) of the title compound are obtained as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255330B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-aa451da6d0274600996a1144b232d4b4 |
| Source note | uspto-grants-2001_07 |