Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Reactant | HCID 70240479 | HCID 70240479 | — |
| Product | HCID 70240411 | HCID 70240411 | 96% |
Reaction Steps
The title compound (70 mg, 96%) was prepared in the same manner as in Example A3, except that the compound (60 mg, 0.19 mmol) prepared in Example A2, anhydrous pyridine (151 μl, 1.87 mmol), and cyclopropanecarbonyl chloride (68 μl, 0.75 mmol) were stirred at 25° C. for 30 min and the purification was performed by column chromatography on silica gel (toluene:ethyl acetate=20:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06255339B1 |
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| Source dataset | uspto-grants-2001_07 |
|---|
| ORD ID | ord-22d6276544b541d391d8d023ac1c67e4 |
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| Source note | uspto-grants-2001_07 |
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