HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1383825Generated: October 25, 2026
Acetic Anhydride → (6-Methylpyridin-2-yl)methyl acetate
https://huagongshe.com/reaction/1383825
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2,6-Dimethylpyridine N-oxide | HCID 14083 | — |
| Product | (6-Methylpyridin-2-yl)methyl acetate | HCID 291137 | — |
Reaction Steps
Acetic anhydride (23 ml) was heated to 110° C. and 2,6-lutidine-N-oxide (20 g) was added dropwise over 1 hour. The solution was heated at 110° C. for five hours. After cooling, the crude mixture was distilled to yield 2-acetoxymethyl-6-methylpyridine (18.4 g, b.p. 110-120° C. @ 15 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06255305B1 |
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| Source dataset | uspto-grants-2001_07 |
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| ORD ID | ord-9d21fda086014f35a60a392747967bee |
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| Source note | uspto-grants-2001_07 |
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