HCID 20669247, compound → 2-(2',4'-Diacetoxyphenyl)propene

Participants

Reaction Steps

Compound (23) (1.7 g, 0.012 mmol) was dissolved in acetic anhydride (3.3 ml), and the solution was stirred for 30 minutes, and refluxed for four hours. The reaction solution was extracted with organic solvent, washed, dried and purified by using column chromatography (eluent: hexane/ethyl acetate=6/1), to obtain 2 g (85%) of pure compound (24).

Provenance & Evidence