HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodododecane → 3-[Dodecyl(methyl)amino]propan-1-OL
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodododecane | HCID 20282 | — |
| Reactant | 3-(Methylamino)-1-propanol | HCID 10148986 | — |
| Product | 3-[Dodecyl(methyl)amino]propan-1-OL | HCID 13122261 | 96% |
Reaction Steps
A solution of 3-(methylamino)propanol (5.71 g, 64.0 mmol, S. Koepke, R. Kupper, and C. J. Michejda, J. Org. Chem., 44, 2718, 1979)), and iodododecane (7.58 g, 25.6 mmol) was reacted as described in example 1 to give 6.33 g (96%) of the title material as an oil, b.p. 100-105° C./0.04 torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255496B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-1647560b948c4231a6a19d7216f8b6f6 |
| Source note | uspto-grants-2001_07 |