HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylbenzoic acid → 2,4,6-Trimethylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylbenzoic acid | HCID 10194 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2,4,6-Trimethylbenzoyl chloride | HCID 97038 | — |
Reaction Steps
A mixture of 328 mg of 2,4,6-trimethylbenzoic acid and 3 mL of thionyl chloride was stirred at room temperature for 2 hours. The volatile components were evaporate in vacuo, the residue was redissolved in 5 mL of CH2Cl2, and the volatile components were again evaporated in vacuo to give 2,4,6trimethylbenzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06258360B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-8c90d1a690bc489b95d3020c69727a24 |
| Source note | uspto-grants-2001_07 |