HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 21186149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 21186092 | HCID 21186092 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21186149 | HCID 21186149 | — |
Reaction Steps
A mixture of 0.6 g of 1-(2-methoxyphenyl)-4-[(5-phenyl-3-pyridyl)methyl]piperazine [obtainable as described for Example 1], 1.8 g of pyridine hydrochloride and 50 ml of pyridine is boiled for 3 hours. The mixture is cooled and evaporated, and work-up is as usual, yielding 1-(2-hydroxyphenyl)-4-[(5-phenyl-3-pyridyl)methyl]piperazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06258813B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-2ce83b3fa5524b9b963fd6067e1af3a4 |
| Source note | uspto-grants-2001_07 |