Methyl Acrylate → HCID 70223765, compound

HRID 1384160Notes

Reaction equation

HRID 1384160 reaction equation
I[C:2]1[CH:3]=[C:4]([C:8]([C:10]2[C:19]([CH3:20])=[CH:18][C:17]3[C:16]([CH3:22])([CH3:21])[CH2:15][CH2:14][C:13]([CH3:24])([CH3:23])[C:12]=3[CH:11]=2)=[O:9])[CH:5]=[CH:6][CH:7]=1.[C:25]([O:29][CH3:30])(=[O:28])[CH:26]=[CH2:27]>>[CH3:20][C:19]1[C:10]([C:8]([C:4]2[CH:3]=[C:2]([CH:27]=[CH:26][C:25]([O:29][CH3:30])=[O:28])[CH:7]=[CH:6][CH:5]=2)=[O:9])=[CH:11][C:12]2[C:13]([CH3:23])([CH3:24])[CH2:14][CH2:15][C:16]([CH3:22])([CH3:21])[C:17]=2[CH:18]=1

Participants

3

Reactant 2

HCID 7294Methyl AcrylateHCID 15428933HCID 15428933, compound

Product 1

HCID 70223765HCID 70223765, compound

Procedure

In a manner similar to that of Example 1(c) by reaction of 6.54 g (15 mmol) of 3-iodophenyl-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthyl)-methanone with 1.8 ml (19.7 mmol) of methyl acrylate, 6.5 g (100%) of the expected methyl ester are obtained in the form of an orange-coloured oil.

Workup

  1. customare obtained in the form of an orange-coloured oil

Sources & evidence

ORD record
ord-e1d4fd3aa3d344409757fcfd412e16bd
Source dataset
uspto-grants-2001_07
Patent number
US06258775B1

Reaction notes

Loading…