Guanidine Hydrochloride → HCID 178432193, compound

Participants

Reaction Steps

When the method of Inventive Example 17 was repeated using 2-methyl-4-nitro-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridine-3-carboxylic acid (750.1 mg, 3.00 mmol) and guanidine hydrochloride (2.77 g, 29.0 mmol), chlorination of the nitro group occurred at the same time and the title compound (134.5 mg, 16.0%) was obtained as white powder.

Provenance & Evidence