Potassium Carbonate → HCID 178474203, compound

HRID 1384381Notes

Reaction equation

[C:1]([NH:4][C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[CH2:13]([NH:20][OH:21])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.C([O-])([O-])=O.[K+].[K+]>>[CH2:13]([N+:20]([O-:21])=[CH:9][C:8]1[CH:11]=[CH:12][C:5]([NH:4][C:1](=[O:3])[CH3:2])=[CH:6][CH:7]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

Reactant 3

HCID 11430Potassium Carbonate

HCID 739424-Acetamidobenzaldehyde

HCID 2794173Benzylhydroxylamine

Product 1

HCID 178474203HCID 178474203, compound

Procedure

Using 4-acetamidobenzaldehyde and N-benzylhydroxylamine (prepared from the hydrochloride salt by treatment with K2CO3) and following the procedures described herein, the title compound was prepared as a yellow powder, m.p. 230.7-237.7° C.

Sources & evidence

ORD record: ord-373da324b3ad4b56b4313c8569859d7e
Source dataset: uspto-grants-2001_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06258852B1

Reaction notes

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