Tert-Butylamine → HCID 54409688, compound

Participants

Reaction Steps

To a 500 ml round bottom flask containing 1.98 g (0.0064 mole) of (1H-cyclopenta[I] phenanthrene-2-yl) dimethylchlorosilane and 250 ml of hexane was added 2.00 ml (0.0160 mole) of t-butylamine. The reaction mixture was allowed to stir for several days, then filtered using diatomaceous earth filter aid (CeliteTM), washed twice with hexane. The product was isolated by removing residual solvent under reduced pressure. The isolated yield was 1.98 g (88.9 percent).

Provenance & Evidence