HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-chlorobenzyl)-phenylacetamide → HCID 21187008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-chlorobenzyl)-phenylacetamide | HCID 306763 | — |
| Reactant | 2-(4-Methylpiperazin-1-yl)benzaldehyde | HCID 2795566 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21187008 | HCID 21187008 | 24.5% |
Reaction Steps
A mixture of 2-(4-methylpiperazin-1-yl)benzaldehyde (0.091 g, 0.45 mmol), N-(4-chlorobenzyl)-phenylacetamide (0.127 g, 0.49 mmol) and N,N-dimethylformamide (2 mL) was treated with anhydrous sodium methoxide (0.072 g, 1.34 mmol) under a nitrogen atmosphere as above to give the title product as an amorphous solid, (0.029 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06258953B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-9e28617780a942a2ac9f74f9446084b2 |
| Source note | uspto-grants-2001_07 |