HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → [2-(2-Thienyl)ethylamino](2-chlorophenyl)acetamide hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | [2-(2-Thienyl)ethylamino](2-chlorophenyl)acetamide | HCID 9882604 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | [2-(2-Thienyl)ethylamino](2-chlorophenyl)acetamide hydrobromide | HCID 21187054 | — |
Reaction Steps
14.7 g (0.05 mol) of [2-(2-thienyl)ethylamino](2-chlorophenyl)acetamide, prepared as described in Example 7, is dissolve din 150 ml of acetone. To the solution 4 ml of 60% aqueous hydrogen bromide solution is added and the precipitated white crystals are filtered off, washed with acetone and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06258961B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-3aa938a98c254de18ce0bedfd69008d4 |
| Source note | uspto-grants-2001_07 |