HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1384495Generated: October 26, 2026
Phenylhydrazine → 2-(Phenylhydrazino)succinonitrile
https://huagongshe.com/reaction/1384495
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | Fumaronitrile | HCID 637930 | — |
| Product | 2-(Phenylhydrazino)succinonitrile | HCID 53865485 | 45% |
Reaction Steps
A mixture of phenylhydrazine (4.29 g) and fumaronitrile (3.1 g), where the phenylhydrazine served as a solvent, was heated at 75-80° C. for 20 hours. Purification by flash chromatography on silica gel and crystallization from dichloromethane/hexane gave the title compound (3.29 g, 45%), m.p. 97-98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06258973B1 |
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| Source dataset | uspto-grants-2001_07 |
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| ORD ID | ord-f98160595e9245248d25f1cf5d0add2f |
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| Source note | uspto-grants-2001_07 |
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