HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → 1-[2-(5-Methyl-4-oxo-3-phenyl-3,5-dihydro-4H-pyridazino[4,5-b]indol-1-yl)-1-oxoethyl]pyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 21183746 | HCID 21183746 | — |
| Product | 1-[2-(5-Methyl-4-oxo-3-phenyl-3,5-dihydro-4H-pyridazino[4,5-b]indol-1-yl)-1-oxoethyl]pyrrolidine | HCID 21183751 | — |
Reaction Steps
The preparation is carried out as in Example 3.2, from 1 g (3 mmol) of 5-methyl-4-oxo-3-phenyl-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-acetic acid and from excess pyrrolidine. The product is recrystallized from propan-2-ol. 0.5 g (1.3 mmol) of solid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262045B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-f9523e29bbe249199e85b34f3e757d9e |
| Source note | uspto-grants-2001_07 |