HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14039945, compound → HCID 14039941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14039945 | HCID 14039945 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14039941 | HCID 14039941 | 50% |
Reaction Steps
Cis-(+)-7-hydroxy-4-phenethyl-1,2,3,4,4a,5,6, 10b-octahydrobenzo[f]quinoline (hereinafter, “cis-(+)-25”) was prepared in 50% yield from 37 mg (0.12 mmole) of cis-(+)-24 by the method of forming trans-9 as described in Example 3. The melting point observed was 194° C. and [α]D (20° C.) was +6.05 (c 0.22, MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262064B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-2580bcba933848728bd95dd17d93f62d |
| Source note | uspto-grants-2001_07 |