HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14039945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 67192496 | HCID 67192496 | — |
| Product | HCID 14039945 | HCID 14039945 | 46% |
Reaction Steps
Cis-(−)-7-hydroxy4-phenethyl-1,2,3,4,4a,5,6, 10b)-octahydrobenzo[f]quinoline (hereinafter, “cis-(−)-25”) was prepared in 46% yield from 34 mg (0.11 mmole) of cis-(−-24 by the method described for trans-9 in Example 3. The melting point observed was 196° C. and [α]D (20° C.) was −6.0 (c 0.20, MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262064B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-c601850acf95455c8ad41d84aa06ff6f |
| Source note | uspto-grants-2001_07 |