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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1384880Generated: October 31, 2026

Methanol → HCID 14039945, compound

https://huagongshe.com/reaction/1384880

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 67192496HCID 67192496—
ProductHCID 14039945HCID 1403994546%

Reaction Steps

Cis-(−)-7-hydroxy4-phenethyl-1,2,3,4,4a,5,6, 10b)-octahydrobenzo[f]quinoline (hereinafter, “cis-(−)-25”) was prepared in 46% yield from 34 mg (0.11 mmole) of cis-(−-24 by the method described for trans-9 in Example 3. The melting point observed was 196° C. and [α]D (20° C.) was −6.0 (c 0.20, MeOH).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06262064B1
Source datasetuspto-grants-2001_07
ORD IDord-c601850acf95455c8ad41d84aa06ff6f
Source noteuspto-grants-2001_07