HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70238476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15895218 | HCID 15895218 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 70238476 | HCID 70238476 | 94.5% |
Reaction Steps
The (S)-3-(4-bromo-2,6-dimethylphenoxymethyl)piperidine in ether was treated with 1M solution of hydrochloric acid in ether (102 mL). The resulting white precipitate was filtered, and dried in vacuo to yield (S)-3-(4-bromo-2,6-dimethylphenoxymethyl)-piperidine hydrochloride (29.5 g, 94.5%), m.p. >280° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262078B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-56febc675637467d8f47c36e530ccb08 |
| Source note | uspto-grants-2001_07 |