HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21184182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21184172 | HCID 21184172 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21184182 | HCID 21184182 | 71% |
Reaction Steps
The 3-(2,6-dimethylphenoxymethyl)-1-(2-dimethylaminoethyl)piperidine solution was treated with a 1M solution of hydrochloric acid in ether (17.2 mL). The resulting precipitate was isolated by filtration, then dried under vacuum to give 3-(2,6-dimethylphenoxymethyl)-1-(2-dimethylaminoethyl)-piperidine hydrochloride (4.0 g, 71%), m.p. 263.2-263.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262078B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-77254c2d3a6c43e5a2e56ab1908ede77 |
| Source note | uspto-grants-2001_07 |