HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinemethanamine → HCID 15547422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinemethanamine | HCID 77317 | — |
| Reactant | HCID 15545850 | HCID 15545850 | — |
| Product | HCID 15547422 | HCID 15547422 | 20.3% |
Reaction Steps
This compound was prepared according to the method of Example 15, using 51 mg (0.184 mmol, 1.0 equiv) 1-cyclopentyl-3-ethyl-1H-indazole-6-carbonyl chloride and 20 μL (0.193 mmol, 1.05 equiv) 4-(aminomethyl)pyridine as starting materials, to give 13 mg (20%) of white crystals: mp 147-149° C.; HRMS calcd for C21H24N4O+H: 349.2028. Found: 349.2031.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-5e0db419a1294ee992100b2a9d2dd6ad |
| Source note | uspto-grants-2001_07 |